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High Pressure Tube Furnace with Ø60 or Ø 80 Alloy Tube (900C or 1100C max heat temp.) - OTF-1200X-HPV

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2-4 weeks to delivery for QC

Product Options

Process Vessel:

OTF-1200X series high-pressure split tube furnaces can be chosen from two kinds of alloy tubes, e.g. Stainless steel 310S refractory alloy or Ni-based superalloy, which offer a solution of heating treatment under high positive pressure with/without inert gas support to process special compound material. The furnace can be heated up to the max. 900°C or 1100°C with the optional vessel. The operating positive pressure is from 105 to 800 psi according to different heating temperatures.
  • Heating temperature up to max. 900°C or 1100°C, Depending on the tube alloy
  • Stainless steel or nickel-base superalloy processing tube is included ( please choose from product optional )
  • Max pressure up to 800 PSI.depended on tube alloy
  • The pressure sensor is installed in the flange. The pressure will be displayed in the pressure controller in the front panel of the furnace. The alarm system is built in the pressure controller. When the pressure exceeds the limit point, the alarm will be activated to release the pressure. 
  • The furnace is able to be controlled by a computer. And the software and USB cable are included
SPECIFICATIONS

OTF1200XHVSS80(60) OTF1200XHPGH60
Process Vessels (Pls select the tube size in the options bar)
SS310S Stainless Steel alloy
80mm O.D x 70(±2) mm I.D x 1000 mm L or 60mm O.D x 50(±2) x 1000 mm L

Ni-based superalloy  (Click to download the alloy datasheet
OD 60 x  ID 52 x  Length 1000 (mm) 
 
Copper gasket

For 80mm O.D tube:
99 O.D x 82 I.D x 2.2mm
For 60mm O.D tube:
82 O.D x 63.6 I.D x 2.2mm
For 60mm O.D tube:
82 O.D x 63.6 I.D x 2.2mm
Working Pressure vs. Working Temperature
 
  600 PSI max   at ≤500°C
  511 PSI max   at ≤600°C
  428 PSI max   at ≤700°C
  203 PSI max.  at ≤800°C
  116 PSI max   at ≤900°C
Attention: Never heat up above 900°
900°C max.for < 1hr  
580 PSI (4 Mpa)     max. at  ≤800°C
362 PSI (2.5 Mpa)   max. at  ≤900°C
174 PSI (1.2Mpa)    max. at ≤1000°C
116 PSI (0.8 Mpa)      max. at 1100°C
Attention: Never heat up above 1100°C
The furnace also can reach high vacuum up to 10-6 torr by turbopump.
Pressure Range
0~15Mpa
0~15Mpa
Max. Heating Temp. 900°C 1100°C
Working Gases
Inert gas & Hydrogen
The inert gas, hydrogen, and oxygen
Heating Temperature
900°C max.for < 1hr  
800°C continuous
1100°C max.for < 1hr 
1000C for continuous
Heating Rate
≤30°C/min ≤20°C/min
Heating Element
Fe-Cr-Al Alloy doped by Mo Fe-Cr-Al Alloy doped by Mo
Heating Zone
Total length: 440mm Single zone
Constant temp. zone: 150mm ±1°C
Total length: 440mm Single zone
Constant temp. zone: 150mm ±1°C
Temp.  Control 

PID control method with over-temp protection
Temperature stability: ±1°C
Demo video here)

PID control method with over-temp protection
Temperature stability: ±1°C
Demo video here)

Thermocouple
 

Omega 3mm OD K Type with high-temperature tolerance (220°C) connector

Omega 3mm OD K Type with high-temperature tolerance (220°C) connector
Positive Pressure Sensor
Installed in the high-pressure flange Installed in the high-pressure flange
PC Control 
(Optional)



Pressure Alarm System
The upper limit and lower limit control method
Alarm strobe and warning whistle
The upper limit and lower limit control method
Alarm strobe and warning whistle
Voltage
AC 220V 50/60Hz
AC 220V 50/60Hz
Power
2.5KW
(20A breaker required)
2.5KW
(20A breaker required)
Dimensions

Closed Cover:   850 x 450 x 540 mm (L x D x H)
Opened Cover: 850 x 600 x 770 mm (L x D x H)


Application Notes
  • The heating temperature must be limited by a certain pressure level due to vessel material strength. Please refer to the specifications
  • The pressure increases while the temperature is rising during operation. So you need to calculate the pressure changing towards your target temperature and set a safe value of pressure during the process
  • The furnace uses a tube with conflate-designed flanges.   
  • The safety pressure relief valve is available to be installed at the downstream side. Please click here for details. 
  • Small quartz or Alumina boat should be used to load the sample into the vessel. Please click the link below to order separately. Never place the sample directly onto the vessel without a crucible. Vessel service life could be reduced significantly if you do so.
  • You may use gold or nickel foil to wrap the crucible boat to minimize the contamination to the pressure vessel.
  •     
  • Optional torque wrench is available here to avoid overtightening the flange bolts
  •    
  • To measure the electric properties of thermoelectric ceramics under high pressure & temperature conditions, please order an alumina testing fixture and high-pressure electrical feedthrough (10Mpa Max.) with the furnace (additional fee will apply).
  •  


Safety Note
  • Ni-based Superalloy ( Waspaloy or equivalent) is a reliable processing tube that can be used under high temperatures and high pressure. It has excellent ductility and tensile property so only creep deformation happens under the overpressure destruction test and is followed by a crack formed (usually at the hot zone at the center of the tube) to release the pressure. Brittle fracture won’t happen in the overpressure destruction test which means no tube explosion will happen under the overpressure of inert gas or safe gas or under other accidents causing overpressure of inert gas or safe gas.
            The pics show a Ni-based Superalloy tube under an overpressure test
  • Attention:  For the use with flammable, toxic, or corrosive gas, you must contact MTI engineering group for the consultation to know all the prerequisites and precautionary measures.
  • Attention A two-stage pressure regulator must be installed on the gas cylinder to limit the pressure to below 3 PSI for safe operation. Please click here to learn how to install the gas regulator.
  • Do not over tightening the flange screws as this may cause permanent damages to the flange or screws. Please refer to the instructions about proper torque for installing CF flange bolts. We recommend you use a torque wrench to tighten the screws with the flange.
Operation Instructions                                       
Warranty One-year limited manufacturer warranty with lifetime support (Consumable parts such as processing tubes, o-rings, and halogen lamps are not covered by the warranty, please order replacements at related products below).

STANDARD PACKAGE
P/N
Name
Qty
OTF1200XHPSS60 OTF1200XHVSS80 OTF1200XHPGH60

Tube Furnace main machine
1

Processing vessel
1
SS310S alloy - 60
SS310S alloy  - 80
Ni-based alloy-60

High-pressure flange set (1 pair)
1
ORing-Cu82 Oxygen-free copper gasket
3
MTS02 USB cable and software for temp management
1
FLG-kit-2 Furnace hook
1

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1. Prices listed online are valid for the US market and who pay by credit card only. There will be extra charges for shipping & handling. Prices vary from country to country.
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